Principle
A fluid must be superheated above its saturation temperature for nucleate boiling to occur. The amount of liquid superheat sustainable is influenced by the presence (or absence) of nucleation sites.
Object
To measure the superheat required to boil water for containers having different surface characteristics.
Background
At one atmosphere pressure, the saturation temperature of water is 100 °C. When a pan of water is heated to 100 °C on an electric heating element, you will observe columns of steam bubbles rising from the base surface of the container. This is nucleate boiling. However, the water in the thin thermal boundary layer near the heating surface is superheated to a temperature greater than 100 °C. Thus, its temperature is greater than the 100 °C saturation temperature.
This experiment demonstrates the degree to which water may be superheated, and the effect of “nucleation sites” in the container wall on the amount of superheating that occurs.
A microwave oven is used for the experiment, because the microwave supplies approximately uniform heat per unit volume to the water.
Apparatus
One litre of degassed water
A clear glass beaker
A microwave oven
A thermocouple to measure the water temperature
A handful of clean sand, or other insoluble granular material
Procedure
The water is first “degassed” by vigorously boiling it in a pan, using a surface heating unit.