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The programme of radiocarbon dating undertaken at Stanwick, Northamptonshire, demonstrates the value of scientific dating of Romano-British sites, including those with good pottery sequences and large numbers of datable coins and other finds. It has refined and clarified the chronology and phasing of the site, particularly in its final phase of occupation. It confirmed some of our original dating of the human burials, and showed other dates were significantly wrong. It also addresses issues relating to the calibration of radiocarbon dates and dietary isotopes in the period. This has enabled us to identify activities, material culture and burial practices current at Stanwick and elsewhere in the immediate post-Roman period.
The use of ultrafiltration remains a subject of ongoing debate among pretreatment methods employed in radiocarbon dating of mammalian archaeological bone. However, such discourse had not previously extended to the archaeology of the Canary Islands (Spain), where detailed descriptions of laboratory processing methods for collagen purification often remain absent. Our study presents a case study involving a new set of radiocarbon dates obtained from the remains of ancient natives of Tenerife Island. For the first time in this region, we compared the results of ultrafiltered with non-ultrafiltered collagen from the same individuals, focusing on the method’s implications for dating accuracy in the Canaries. Through an examination of the cleaning protocols of ultrafilters and an assessment of the reliability of radiocarbon dating outcomes, we have found that ultrafiltration may influence the accuracy of results. However, given the additional handling required and the potential risk of contaminating the samples, its application should be carefully considered. In the context of the Canary Islands, ultrafiltration may be most relevant for samples associated with early human occupation, though further research is needed to assess its necessity across different biogeographical contexts. This communication further contributes to a broader understanding of preparation methods for radiocarbon dating bone from various environmental contexts, emphasizing the uniqueness of each case. Furthermore, we discuss the implications of our findings for archaeological research in the Canary Islands, highlighting the methodological gaps that persist in the region and underscoring the importance of ensuring the accuracy and reliability of chronological interpretations in archaeological investigations.
We report a new relative sea level curve from Inglefield Land, northwest Greenland, to investigate the transition from maximum to minimum loading across Nares Strait. We sampled marine bivalves and terrestrial macrofossils for radiocarbon dating from raised marine terraces in Rensselaer Valley, Inglefield Land (78.58°N, 70.71°W) to constrain relative sea level through the Holocene. The oldest terrestrial macrofossil of 9010–8650 cal yr BP provides a minimum-limiting constraint for the deglaciation. Sea level fell rapidly from the marine limit at 85 ± 4 m to 37.5 ± 4 m above sea level (m asl) between 9010–8650 and 7970–7790 cal yr BP at a rate of 49 m/ka. The rate of sea -level fall decreased to 11 m/ka between 7970–7790 and 5320–5060 cal yr BP, when it fell from 37.5 ± 4 to 9 ± 4 m asl. After 5,320–5,060 cal yr BP, we estimate sea level fell at a lower rate of 2 m/ka to modern sea level. The period of fastest emergence in Inglefield Land is earlier in time than in Hall Land, reflecting earlier deglaciation, and is steeper than in Hall Land and Washington Land. This sea-level history captures the transition from the style of emergence from Pituffik to Hall Land.
We investigated radiocarbon dates of human bone samples from several medieval sites in Trondheim, central Norway. Stable isotope data was used to estimate marine correction for the radiocarbon dates, which is necessary to correct the radiocarbon ages and establish age models for the archaeological layers. We observed that a marine correction without ΔR does not lead to a well-defined model for all sites. Allowing a variable ΔR improves the model, which indicates that food sources and trade routes have changed over time, influencing the mobility of food resources as well as of people. However, this does not work for all sites, indicating that variation of reservoir ages could also be the result of individual preferences for the food and that fish with different ΔR, and thus different geographical origin, was consumed during the same periods. Many radiocarbon and stable isotope (δ13C, δ15N) measurements have been carried out for the project. We calculated %marine consumption from the isotope values and found that it varies greatly, between 7% and 51%, and apparently independent of period, social status, churchyard location or other factors. Based on these data, we determined average reservoir ages for the marine food consumed in Trondheim during different phases, varying between ΔR = –150 and 280 years.
Using calibrated radiocarbon dates, this study investigates climate signals recorded in fluvial sedimentary archives from southern Poland, eastern Netherlands, and eastern Germany. Summed probability density functions (PDFs) were constructed and analyzed in the context of INTIMATE stratigraphy. The results indicate that fluvial sedimentation and erosion processes were closely linked to climate fluctuations, particularly during GS/GI and GI/GS transitions. The analyses indicate multi-scale relationships between regional geomorphological processes and global climate trends during the period from 50 to 15 cal kBP. This study provides a reconstruction of Late Pleistocene fluvial activity and highlights the need for more precise radiocarbon dates to refine correlations between regional and global climate events.
In recent decades, numerous excavations have been conducted at prehistoric sites in northwestern Iran, and the results of these studies have contributed to the development of a chronological framework for the region. The early Chalcolithic period in this area is referred to as the Dalma or Hasanlu X period. Various theories have been proposed regarding the chronological span of this culture, yet challenges and debates about its dating remain. The Belachak 3 site is one of the settlements attributed to this period, excavated by the first author of this article. The excavation results indicate that the site was temporarily occupied. The pottery recovered from this site closely resembles the ceramics found at well-known Dalma sites such as Dalma Tepe and Nad Ali Beig. This article aims first to explore the relative and absolute chronology of the Belachak 3 site. Subsequently, it evaluates the dating of this culture based on the absolute chronology of this and other Chalcolithic sites in western and northwestern Iran. For dating Belachak 3, five animal bones were sent to the Poznań Radiocarbon Laboratory. The results indicate that the site was occupied around 5000–4700 BCE. Additionally, based on the pottery findings and absolute dating, it can be suggested that the Dalma culture likely emerged in the late 6th millennium BCE and became widespread across large areas of western and northwestern Iran from around 5000 BCE onward.
The Salapunku archaeological site is located within the Historic Sanctuary – National Archaeological Park of Machu Picchu (HS-NAPM) in the Cusco area of Peru. Although Salapunku is related to the Inca settlements of the HS-NAPM, during archaeological excavations, we distinguished different moments of cultural occupation from the earliest human presence to complex pre-Hispanic societies such as the Inca and finally to the colonial period. Previous research on the site’s chronology was based on typological analyses of pottery and other artifacts found during archaeological research. This radiocarbon analysis, the first of its kind in this area, establishes a chronology of the cultural history of this significant settlement, considered the gateway to the Cordillera of Vilcabamba.
An increase in knowledge is usually beneficial but can also highlight misapprehensions of existing data. Such is the case for the Pictish-Norse transition in Northern Scotland in the later first millennium AD. New radiocarbon dates from the key ‘transitional’ settlement of Buckquoy, Orkney, reveal that traits previously published as indicative of incoming Norse influence pre-date the start of the Viking Age, suggesting a greater level of endogenous change than hitherto has been appreciated. Here, the authors underscore the need for a re-evaluation of other settlement sequences across the later Pictish and early Norse periods, reopening many questions about the transition.
How old is the Grand Canyon? When did the glaciers last retreat from this area? How long does it take to form an inch of topsoil? When did the earthquake occur that formed these rock scarps? These are the questions that geomorphologists ponder. This chapter will outline the tools and approaches we use to answer such questions.
Establishing how old a landform might be, that is, when it formed, has always occupied the mindset of geomorphologists. If we know how OLD a landform is, then we can begin to understand how it is evolving, how fast it might be changing, and how it formed in the first place. Fortunately, various dating principles and techniques now exist to address these issues. These techniques require the ability to measure change in a system or a landform over time, with the (usual) goal of establishing the age of a sediment package or a landform.
The Darband Wall in southern Uzbekistan marks an important political border in the Classical world, yet the dating of its construction is largely relative and contested. Presenting 10 new radiocarbon dates from the wall, the authors argue that construction began in the early or middle third century BC, likely under Seleucid or early Greco-Bactrian rule, while later reconstruction efforts coincide with Kushan expansion around the first and second centuries AD. Early Hellenistic-style fortifications reveal a defensive, and possibly an orientational, shift during Kushan rule that underscores both the strategic significance of the wall and the need for more extensive investigation.
The emergence, on the Loess Plateau of Central China, of settlements enclosed by circular ditches has engendered lively debate about the function of these (often extensive) ditch systems. Here, the authors report on a suite of new dates and sedimentological analyses from the late Yangshao (5300–4800 BP) triple-ditch system at the Shuanghuaishu site, Henan Province. Exploitation of natural topographic variations, and evidence for ditch maintenance and varied water flows, suggests a key function in hydrological management, while temporal overlap in the use of these three ditches reveals the large scale of this endeavour to adapt to the pressures of the natural environment.
This study from the Accelerator Mass Spectrometry Laboratory at the Center for Physical Sciences and Technology (FTMC), Vilnius, Lithuania, presents a detailed description of the sample preparation methods employed in the laboratory, with a focus on two AMS systems: a single-stage accelerator mass spectrometer (SSAMS) and a low energy accelerator (LEA). A pivotal aspect of this article is our participation in the GIRI intercomparison test, demonstrating our commitment to precision and accuracy in radiocarbon dating, with the average z-score values of the GIRI test being 0.16 ± 1.66 for SSAMS and –0.04 ± 1.52 for LEA. The outcomes from this participation validate the meticulous sample preparation procedures at Vilnius Accelerator Mass Spectrometry Laboratory and offer significant insights into the efficiency and reliability of SSAMS and LEA systems, contributing to a better understanding of their capabilities in radiocarbon analysis.
The Đurđevac Sands constitute a wide area of small-scale dune relief in the Podravina (NE Croatia), located along the central part of the southern Drava River valley. Even though it has been the subject of earlier investigations, the timing and characteristics of aeolian activity and pedogenesis remain unclear. In this study, field investigations and laboratory methods are combined to gather information on past aeolian systems in the southern part of the Pannonian Basin. The results indicate that weak soil formation during the Bølling-Allerød interstadial stabilized the dunes after the first episode of aeolian activity that took place since ca. 18 ka. The source material for dune building is thought to be fluvial sand from the Drava River, which was blown from exposed terraces. During the Younger Dryas and/or Early Holocene, a new phase of aeolian activity is recorded, with material showing stronger evidence of weathering compared to the underlying aeolian material. Finally, during the Mid and/or Late Holocene, dunes were overbuilt once again with fresh unweathered sand. In general, these new findings obtained from the Đurđevac Sands area correlate rather well with other regions in the Pannonian Basin, in terms of the timing and characteristics of soil formation and aeolian activity.
This study applies Bayesian chronological modeling to 16 new AMS radiocarbon dates on short-lived botanical remains and wood-charcoal recovered from the archaeological site Ahatsistari, a seventeenth-century Huron-Wendat village located in Simcoe County in Ontario, Canada. The modeled radiocarbon dates provide an independent time frame for understanding site phase and sequence, compatibility with historically documented events of a known date, and assessment of the socioeconomic and political influences affecting the composition of European trade good assemblages from different sites. We argue that Ahatsistari is likely Carhagouha, the principal village of the northern Attignawantan who were members of the Huron-Wendat Confederacy, and home to Samuel de Champlain and Joseph Le Caron from 1615 to 1616. In addition, Ahatsistari is contemporary with the archaeological site Warminster, which is believed to be Champlain’s Cahiagué. Radiocarbon dates from the archaeological sites of Ahatsistari, Warminster, and Ball are consistent with earlier suppositions for the beginning and end of Glass Bead Period 2 (AD 1600–1625), whereas differences in the composition of the glass trade bead assemblages speak to the prominent role of Ahatsistari in trade with the French and to variable trade relations among other early seventeenth-century Huron-Wendat villages.
Cemeteries of the Early Neolithic Linearbandkeramik culture (LBK, 5500–4900 BC) evoke a sense of emerging permanence of place as agricultural subsistence spread westward through Central Europe. Yet assumptions about the sequence of senescence and longevity of cemetery use are based on limited data. Here, the authors challenge the view that cemetery burial was a long-lasting Neolithic practice, modelling 50 new radiocarbon dates from the cemetery of Schwetzingen alongside published dates from eight other LBK mortuary contexts. The results, they argue, indicate a short-lived, largely contemporaneous cemetery horizon across Central Europe, forcing a re-evaluation of Early Neolithic social history.
The Tupí linguistic group is one of the most widespread in South America, indicating a deep history of population movement, yet the ancestral homeland and migration routes of descendant groups remain the subject of debate due to the fragmentary nature of the Amazonian archaeological record. Using a database of more than 660 georeferenced dates from sites of the Tupinambá and Guaraní peoples, the authors deploy a mobility model to investigate the timing of population movements, viable routes and the distances achieved. The results create a more nuanced understanding of the rhythms of migration through an ecologically and socially complex landscape.
In this study, we investigate the impact of X-rays produced by conventional mCT instruments on fossil materials dated by radiocarbon. Our results clearly show a decrease on the collagen preservation in fossil and modern bones and teeth, and therefore on the radiocarbon analytical results (in particular, the collagen yield and, possibly, stable isotope composition), after mCT scanning. In other words, all the samples analysed here have experienced a noticeable radiation damage, regardless of their nature (bone and dental tissue) and age (modern and fossil). Given these observations, a prudent approach would be for radiocarbon laboratories to expect lower collagen yields for samples that have been previously mCT scanned and ensure appropriately sized standards are processed alongside these samples. Additionally, samples with originally low collagen yields might become unsuitable for radiocarbon dating after mCT or at least show a yield lower than the usual minimum cut-off value. In this case, it might be viable to extend the collagen yield quality assurance parameter for mCT scanned bones and teeth and instead focus on the C:N ratio as the most appropriate indicator of collagen quality, although we cannot exclude that the latter may also be impacted by X-ray exposure. Further investigations on a larger set of samples are required to confirm these first observations. Nevertheless, in the light of these results, we can reasonably conclude by recommending caution regarding the systematic and unlimited use of mCT scanning in palaeoanthropology or in other related disciplines involving fossil material.
As with the peopling of the Pacific Islands, the monumental ritual architecture of East Polynesia is presumed to have spread from West Polynesia. By re-examining the wealth of absolute dates available from ritual contexts across these diverse islands, the authors challenge this generalisation in Polynesian ideological materialisation, identifying three phases of development. They argue that initial west-to-east migration spread the concept of ritual spaces marked by stone uprights c. AD 1000–1300, then the formalisation of monuments diffused in the opposite direction c. AD 1300–1600, before megastructures emerged from localised hierarchisation, perhaps earliest on Rapa Nui c. AD 1350–1500.
Despite an early surge in copper-ore mining during the sixth and fifth millennia BC (the ‘boom’), evidence for metal production in the Balkans dwindles in the fourth millennium (the ‘bust’). Here, the authors present new evidence for copper mining at Curak in south-west Serbia, c. 3800 cal BC, during this apparent downturn. By integrating field surveys, excavations and provenance analyses, they explore activity at the site, challenging the visibility bias in the archaeological record of this region for this key period. Rather than a societal collapse, the authors argue, fewer artefacts may instead reflect a widening Balkan sphere of influence.
Ice-sheet volume during Marine Isotope Stage (MIS) 3 (57–29 ka) is controversial. Several recent studies have proposed that the Greenland Ice Sheet was smaller during MIS 3 than it is today based on radiocarbon ages of molluscan bivalve shells reworked into sedimentary deposits adjacent to the present ice margin. Such a result contrasts with available records of MIS 3 climate, ice volume, and sea level. We revisited a site previously interpreted as containing evidence for smaller than present ice during MIS 3. We collected marine bivalve shells and combined progressive acid dissolution in preparation for radiocarbon dating with new-generation amino acid analysis, which focuses on aspartic acid racemization. Our results suggest that contamination by young carbon yields finite radiocarbon ages despite bivalve shells likely dating to MIS 5e (∼125 ka) or even older. This result should be further tested, which could be accomplished with additional studies of this kind in combination with ice-sheet modeling and additional paleoclimate data generated from adjacent seas.