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X-ray Powder Data for Sodium tri-aqua-hexa-(nicotinato-tri-μ-oxo- tri-chromium (III) perchlorate) hexahydrate {Na [Cr3O(C6H5NO2)6 (H2O)3] [ClO4]8·C6H5NO2·6H2O}

Published online by Cambridge University Press:  10 January 2013

D. F. Mullica ,
E. L. Sappenfield  and
J. E. Bradshaw
D. F. Mullica
Affiliation:
Chemistry and Physics Departments, Baylor University, Waco, Texas 76798
E. L. Sappenfield
Affiliation:
Chemistry and Physics Departments, Baylor University, Waco, Texas 76798
J. E. Bradshaw
Affiliation:
Chemistry and Physics Departments, Baylor University, Waco, Texas 76798
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Abstract

The indexed X-ray diffraction powder data of sodium triaqua-hexa-(nicotinato-tri-μ-oxo-tri-chromium(III) perchlorate) hexahydrate {Na [Cr3 O(C6H5NO2)6(H2 O)3] [ClO4]8·C6H5NO2·6H2O, NICCR} is reported. NICCR crystallizes in the hexagonal space group P63/m. The refined cell parameters were determined by employing a Siemens Debye-Scherrer camera (Fe Kā radiation, λmean= 1.93736 Å). The cell constants are a = 13.573(2), c = 24.901(5) Å, V = 3972.8 Å3 and Dx =1.68 Mg m-3 (Dm =1.67 Mg m-3). The quantitative figure of merit (FN) for NICCR is F27 = 32(0.010,81). The JCPDS Diffraction File No. is 36–1978.

Information

Type
Research Article
Information
Powder Diffraction , Volume 1 , Issue 3 , September 1986 , pp. 261 - 262
Copyright
Copyright © Cambridge University Press 1986

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