Hostname: page-component-745bb68f8f-hvd4g Total loading time: 0 Render date: 2025-02-04T16:49:34.603Z Has data issue: false hasContentIssue false
  • English
  • Français

A Microscopic Marker Technique For Documenting Interface Motion in Corrosion Scales Using TEM

Published online by Cambridge University Press:  21 February 2011

Shou-Kong Fan  and
Linn W. Hobbs
Shou-Kong Fan
Affiliation:
Department of Materials Science and Engineering, M.I.T., Cambridge, MA 02139 now at Texas Instruments, Inc., P.O. Box 655621, Dallas, TX 75265
Linn W. Hobbs
Affiliation:
Department of Materials Science and Engineering, M.I.T., Cambridge, MA 02139
Get access

Abstract

We report here on a microscopic marker technique designed for use with cross-section TEM examination of corrosion scales. The technique involves microphotolithographic methods for sputter deposition of inert markers and has been used to document substrate/scale interface motion during high-temperature oxidation of Ni and Ni-base alloys.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 115: Symposium W – Specimen Preparation for Transmission Electron Microscopy of Materials I , 1987 , 283
Copyright
Copyright © Materials Research Society 1988

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Smielgas, A. and Kirkendall, E., Trans. AIME 171, 130 (1947); J. A. Sartell and C. H. Li, J. Inst. Metals 90, 92 (1961).Google Scholar
2. Hobbs, L. W. and Mitchell, T. E., in High Temperature Corrosion, ed. Rapp, R. A. (NACE, Houston, TX, 1983), pp. 76–83.Google Scholar
3. Marcus, R. B. and Sheng, T. T., Transmission Electron Microscopy of Silicon VLSI Circuits and Structures (John Wiley & Sons, New York, 1983).Google Scholar
4. Hindam, H. M. and Smeltzer, W. W., Oxid. Metals 14, 337 (1980).Google Scholar
5. Hobbs, L. W., Sawhill, H. T. and Tinker, M. T., Trans. Jap. Inst. Metals 24 (JIMIS-3 Supplement), 115–20 (1983); H. T. Sawhill and L. W. Hobbs, in Proc. Intl. Cong. on Metallic Corrosion (National Research Council of Canada, Ottawa, 1984), Vol. 1, pp. 21–26.Google Scholar