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Published online by Cambridge University Press: 26 February 2011
An atomic model of the structure of a <001> ∑ = 13 grain boundary is proposed. The segregation of cobalt at the same grain boundary is investigated by M∑ϐbauer spectroscopy, autoradiography and the I6/I14 method quantitatively. The results, which are consistent with the assumption that CoSi2 precipitates are formed, are discussed in view of the atomic structure.