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Published online by Cambridge University Press: 22 February 2011
By exciting diffraction in the Laue geometry by specularly reflected beams, penetrating x-rays and neutrons can be used to probe surface and interfacial atomic structure. We present the first such measurement utilizing polarized neutrons with both incident- and exit-angle resolution. We have observed the evolution of magnetic order by monitoring the in-plane (1010) Bragg peak from an epitaxially grown film consisting of 150 Å Y(0001) on 5000 Å Gd(0001). Magnetic scattering increases as the film is cooled from the Gd bulk Curie temperature (293K) to 100 K. The gross features of the data can be captured by a simple two-layer model, but sufficient disagreement remains that one may yet hope to extract non-trivial structure at the Y/Gd interface.