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SERS properties of biogenic gold nanoparticles synthesized using Anemopsis californica extract.

Published online by Cambridge University Press:  26 November 2020

R. D. Ávila-Avilés ,
Marco A. Camacho-López ,
E. Castro-Longoria ,
A. Dorazco-González ,
N. Hernández-Guerrero  and
A. R. Vilchis-Nestor Open the ORCID record for A. R. Vilchis-Nestor [Opens in a new window]
R. D. Ávila-Avilés
Affiliation:
Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM, Highway Km. 14.5, San Cayetano, Toluca - Atlacomulco, 50200, Toluca de Lerdo, México. Departamento de Genética y Biología Molecular CINVESTAV-IPN, Av Instituto Politécnico Nacional 2508, 07360, Ciudad de México, México.
Marco A. Camacho-López
Affiliation:
LIDMA, Facultad de Química, Universidad Autónoma del Estado de México, Campus Rosedal, Km 14.5 Carretera Toluca-Atlacomulco, San Cayetano de Morelos, Toluca C.P. 50295, México.
E. Castro-Longoria
Affiliation:
Departamento de Microbiología, CICESE, Ensenada, B.C., México, CP 22860.
A. Dorazco-González
Affiliation:
Instituto de Química, Universidad Nacional Autónoma de México, Ciudad Universitaria, Coyoacán, Ciudad de México, C.P. 04510, México.
N. Hernández-Guerrero
Affiliation:
Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM, Highway Km. 14.5, San Cayetano, Toluca - Atlacomulco, 50200, Toluca de Lerdo, México.
A. R. Vilchis-Nestor*
Affiliation:
Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM, Highway Km. 14.5, San Cayetano, Toluca - Atlacomulco, 50200, Toluca de Lerdo, México.
*
*corresponding author
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Abstract

Gold nanoparticles (AuNPs) have been classified as one of the most attractive nanotechnologies, thanks to their potential or already implemented applications; therefore, biological methods for their synthesis have been widely investigated. This study explores the synthesis of AuNPs using the extract of Anemopsis californica, and determinates the effect of the solvent used (water, methanol, and isopropanol) to obtain the AuNPs. Biogenic nanoparticles were analysed through UV-Vis spectroscopy and transmission electron microscopy (TEM, HRTEM, and SAED). Significant differences in polydispersity and morphology of AuNPs among the different methods used were found; the aqueous extract and the extract based on methanol formed nanotriangles and polyhedral nanoparticles; the shape of the nanoparticles is predominantly polyhedral when isopropanol is used as the solvent. The as obtained nanoparticles were placed on glass slides to perform Surface-Enhanced Raman Scattering (SERS) experiments, an amplification of the methylene blue Raman signal was observed when triangular nanoparticles cover the biogenic SERS substrate.

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Articles
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MRS Advances , Volume 5 , Issue 63: International Materials Research Congress XXIX , 2020 , pp. 3397 - 3406
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Copyright © The Author(s), 2020, published on behalf of Materials Research Society by Cambridge University Press

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