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Effects of Glass Elements on the Structural Evolution of in situ Grown Ferroelectric Perovskite Crystals in Sol-gel Derived Glass-ceramics

Published online by Cambridge University Press:  31 January 2011

Kui Yao ,
Weiguang Zhu ,
Liangying Zhang  and
Xi Yao
Kui Yao
Affiliation:
Microelectronics Center, School of Electrical and Electronic Engineering, Nanyang Technological University, Singapore 639798
Weiguang Zhu
Affiliation:
Microelectronics Center, School of Electrical and Electronic Engineering, Nanyang Technological University, Singapore 639798
Liangying Zhang
Affiliation:
Electronic Materials Research Laboratory, Xi'an Jiaotong University, Xi'an 710049, China
Xi Yao
Affiliation:
Electronic Materials Research Laboratory, Xi'an Jiaotong University, Xi'an 710049, China
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Abstract

Several ABO3 perovskite ferroelectric crystals, PbTiO3, Pb(Zr, Ti)O3, and BaTiO3 have been in situ grown from amorphous gels with glass elements, and the structural evolution has been systematically investigated using x-ray diffraction (XRD), infrared spectra (IR), differential thermal analysis (DTA), thermogravimetric analysis (TGA), and dielectric measurements. It is found that in the Si-contained glass-ceramic systems, Si and B glass elements are incorporated into the crystalline structures, resulting in the variation of the crystallization process, change of lattice constant, and dielectric properties. Some metastable phases expressed by a general formula AxByGzOw (A = Pb and Ba; B = Zr and Ti; G for glass elements, especially for Si) have been observed and discussed.

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Articles
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Journal of Materials Research , Volume 12 , Issue 4 , April 1997 , pp. 1131 - 1140
Copyright
Copyright © Materials Research Society 1997

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