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Thermal instability of (Bi,Pb)2Sr2Ca2Cu3Ox in contact with silver

Published online by Cambridge University Press:  31 January 2011

Robert J. Moon ,
Kevin P. Trumble  and
Keith J. Bowman
Robert J. Moon
Affiliation:
School of Materials Engineering, Purdue University, West Lafayette,Indiana 47907
Kevin P. Trumble
Affiliation:
School of Materials Engineering, Purdue University, West Lafayette,Indiana 47907
Keith J. Bowman
Affiliation:
School of Materials Engineering, Purdue University, West Lafayette,Indiana 47907
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Abstract

The chemical and microstructural evolution of particulate (Bi,Pb)2223 in contact with pure bulk silver at 830 to 905 °C under flowing air and Ar−5% O2 atmospheres has been studied. Specimens annealed under PO2 and temperature conditions for which the (Bi,Pb)2223 phase itself is stable, based on a critical assessment of the literature, revealed a silver/(Bi,Pb)2223 interface-limited reaction, producing both solid and liquid decomposition phases. The (Bi,Pb)2223 not in direct contact with silver exhibited no reaction under the same conditions. Solid silver dissolves into the (Bi,Pb)2223 incongruent liquid, facilitating the incongruent melting reaction. On cooling, equiaxed metallic silver particles precipitated uniformly throughout bulk specimens partially melted on a silver substrate.

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Articles
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Journal of Materials Research , Volume 14 , Issue 3 , March 1999 , pp. 652 - 664
Copyright
Copyright © Materials Research Society 1999

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