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Rietveld refinement of the crystal structure of α-CoSO4

Published online by Cambridge University Press:  10 January 2013

Peter C. Burns  and
Frank C. Hawthorne
Peter C. Burns
Affiliation:
Department of Geological Sciences, The University of Manitoba, Winnipeg, Manitoba R3T 2N2, Canada
Frank C. Hawthorne
Affiliation:
Department of Geological Sciences, The University of Manitoba, Winnipeg, Manitoba R3T 2N2, Canada
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Abstract

The crystal structure of α-CoSO4 has been refined by the Rietveld method from X-ray powder diffraction data. The structure is orthorhombic, space group Pnma, a = 8.6127(4), b = 6.7058(3), c = 4.7399(2) Å, V = 273.75(3) Å3. Final RB = 2.41%, RP = 5.24%, RWP=6.66%, RWP (expected) =5.74% (WP =weighted profile). The structure consists of edge-sharing octahedral chains parallel to [010] interconnected by SO4 tetrahedra.

Information

Type
Research Article
Information
Powder Diffraction , Volume 8 , Issue 1 , March 1993 , pp. 54 - 56
Copyright
Copyright © Cambridge University Press 1993

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