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Flame Spray Pyrolysis of Electrode Materials for Energy Applications

Published online by Cambridge University Press:  08 April 2015

Paul I. Dahl ,
Magnus S. Thomassen ,
Luis C. Colmenares ,
Alejandro O. Barnett ,
Scott Lomas ,
Per E. Vullum ,
Sidsel M. Hanetho  and
Tommy Mokkelbost
Paul I. Dahl*
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Magnus S. Thomassen
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Luis C. Colmenares
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Alejandro O. Barnett
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Scott Lomas
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Per E. Vullum
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Sidsel M. Hanetho
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
Tommy Mokkelbost
Affiliation:
SINTEF Materials and Chemistry, Trondheim, Norway
*
*Corresponding author: paul.inge.dahl@sintef.no, +47-98243955
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Abstract

Flame spray pyrolysis (FSP) was applied to produce nanopowders of Ti1-xMxO2 and Sn1-xMxO2, where x = 0.05 and M = Nb/Sb, for use as catalyst support materials in PEM fuel cells/ electrolysers. FSP powders in the SnO2-IrO2 system were produced for the same applications. Homogenous particle size distribution (5-20 nm) was demonstrated by TEM, supported by BET and XRD analysis. Whereas two polymorphs were indicated for the Ti-based oxides, the Sb/Nb-doped SnO2 powders were single phase. FSP powders of Mn3O4 intended for supercapacitors were produced and the influence of the precursor/solvent mixtures on the physical and electrochemical properties evaluated.

Keywords

flame synthesisoxidenanoscale

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